Food Contaminants and Residue Analysis
by Picó-
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Summary
Table of Contents
| Contributors to Volume 51 | p. xiii |
| Volumes in the Series | p. xix |
| Preface | p. xxiii |
| Series Editor's Preface | p. xxv |
| Challenges in Chemical Food Contaminants and Residue Analysis | p. 1 |
| Introduction | p. 2 |
| Emerging Contaminants | p. 7 |
| Masked Contaminants | p. 14 |
| Unknown Bioactive Contaminants | p. 15 |
| Emerging Technologies | p. 18 |
| Validation and QA/QC Challenges | p. 22 |
| Conclusions and Future Trends | p. 24 |
| Acknowledgements | p. 25 |
| References | p. 25 |
| International Regulations on Food Contaminants and Residues | p. 29 |
| Introduction to EU and USA Legislation | p. 29 |
| Topics/Categories Covered under EU Legislation | p. 31 |
| Topics/Categories Covered under USA Legislation | p. 63 |
| References | p. 73 |
| Guidelines on Quality Implementation for Analytical Methods | p. 77 |
| Introduction | p. 77 |
| The Role of Quality | p. 78 |
| Conclusions | p. 86 |
| References | p. 87 |
| Immunochemical and Receptor Technologies: The Role of Immunoassay, Immunoaffinity Chromatography, Immunosensors and Molecularly Imprinted Polymeric Sensors | p. 91 |
| Introduction | p. 92 |
| Definitions and Concepts | p. 93 |
| Immunoassay Formats | p. 95 |
| Immunoassay Development | p. 96 |
| Immunochemical Technologies | p. 101 |
| Biomimics: Molecularly Imprinted Polymers (MIPs) | p. 113 |
| Commercial Instrumentation and Future Perspectives | p. 122 |
| References | p. 125 |
| Advanced Sample Preparation Techniques for the Analysis of Food Contaminants and Residues | p. 131 |
| Introduction | p. 131 |
| Sample Preparation Methods for VOCs | p. 133 |
| Sample Preparation Methods for SVOCs and NVOCs | p. 138 |
| Fractionation and Clean-Up | p. 162 |
| Evaporation | p. 170 |
| Derivatization | p. 170 |
| Conclusion | p. 171 |
| References | p. 172 |
| Recent Developments in Chromatographic Techniques | p. 175 |
| Introduction | p. 175 |
| Fast Chromatographic Separation | p. 176 |
| Two-Dimensional Chromatographic Separation | p. 188 |
| Overcoming Adverse Matrix Effects | p. 191 |
| Future Trends | p. 196 |
| References | p. 197 |
| New Approaches in Mass Spectrometry | p. 201 |
| Introduction | p. 201 |
| High Resolution and Accurate Mass Analysers | p. 204 |
| Tandem Mass Spectrometry | p. 211 |
| High Resolution Mass Spectrometers in Tandem | p. 219 |
| Conclusions and Future Trends | p. 227 |
| References | p. 228 |
| Capillary-Based Separation Techniques | p. 231 |
| Introduction | p. 231 |
| Miniaturization and the Capillary Format | p. 232 |
| Capillary Liquid Chromatography | p. 233 |
| Capillary Electroseparations | p. 235 |
| Detection Techniques in Capillary-Based Separations | p. 250 |
| Automation and On-Line/In-Capillary Coupled Solid-Phase Extraction in Capillary Electrophoresis | p. 251 |
| Applications in Determination of Food Contaminants Using Capillary Electrophoresis | p. 252 |
| References | p. 253 |
| Pesticide Residues | p. 257 |
| Introduction | p. 257 |
| Physical and Chemical Properties | p. 258 |
| Health Effects | p. 259 |
| Analytical Methods | p. 272 |
| Instrumental Determination | p. 278 |
| LC-MS-MS Applications | p. 295 |
| Conclusions and Future Trends | p. 301 |
| References | p. 302 |
| Veterinary Drug Residues | p. 307 |
| Introduction | p. 307 |
| Physical and Chemical Properties Affecting Analytical Methodology | p. 313 |
| Human Health Effects from Veterinary Drug Residues | p. 315 |
| Analytical Methods | p. 317 |
| Occurrence in Food | p. 328 |
| Future Trends | p. 329 |
| References | p. 332 |
| Analytical Strategies to Control the Illegal Use of Banned Growth Promoters in Meat Producing Animals | p. 339 |
| Introduction | p. 339 |
| Chemical Properties, Health effects | p. 340 |
| Analytical Methods | p. 342 |
| Occurrence in Foods | p. 357 |
| Future Trends | p. 358 |
| References | p. 358 |
| Mycotoxins | p. 363 |
| Introduction | p. 364 |
| Classes of Mycotoxins | p. 366 |
| Health Effects | p. 376 |
| Sampling | p. 383 |
| Analytical Methods | p. 385 |
| Occurrence in Food and Feed | p. 402 |
| Decontamination Procedures | p. 416 |
| Future Needs | p. 418 |
| Acknowledgement | p. 419 |
| References | p. 419 |
| Phycotoxins | p. 429 |
| Introduction | p. 429 |
| Seafood-Poisoning Toxins | p. 430 |
| Paralytic Shellfish Poisoning (PSP) Toxins | p. 430 |
| Diarrhetic Shellfish Poisoning (DSP) Toxins | p. 432 |
| Azaspiracid Poisoning (AZP) Toxins | p. 439 |
| Amnesic Shellfish Poisoning (ASP) Toxins | p. 442 |
| Yessotoxins (YTXs) | p. 445 |
| Neurotoxin Shellfish Poisoning (NSP) Toxins | p. 448 |
| References | p. 452 |
| Persistent Organochlorine Pollutants, Dioxins and Polychlorinated Biphenyls | p. 457 |
| Introduction | p. 457 |
| Physical and Chemical Properties and Use of POPs | p. 460 |
| Health Effects | p. 462 |
| Analytical Methods | p. 467 |
| Occurrence in Food | p. 495 |
| Future Trends | p. 496 |
| References | p. 498 |
| Brominated Flame Retardants as Food Contaminants | p. 507 |
| Introduction | p. 507 |
| Analytical Methods | p. 512 |
| Occurrence in Food | p. 542 |
| Regulatory/Safety Aspects and On-Going Monitoring Programmes | p. 560 |
| Future Trends in the BFR Research in Food | p. 562 |
| Acknowledgement | p. 563 |
| References | p. 563 |
| Metals | p. 571 |
| Introduction | p. 571 |
| Analytical Procedure for Metal Determination | p. 573 |
| Metals of Interest | p. 585 |
| Directive for Trace Metals in Food | p. 589 |
| Conclusions and Future Trends | p. 589 |
| References | p. 590 |
| Polycyclic Aromatic Hydrocarbons | p. 599 |
| Introduction | p. 599 |
| Physical and Chemical Properties | p. 601 |
| Health Effects | p. 602 |
| Analytical Methods | p. 611 |
| Occurrences of PAHs in Food | p. 632 |
| Future Trend | p. 642 |
| Acknowledgements | p. 644 |
| References | p. 644 |
| Methods for the Determination of N-Nitroso Compounds in Food and Biological Fluids | p. 653 |
| Introduction | p. 654 |
| Physical and Chemical Properties of NOC | p. 656 |
| Health Effects | p. 657 |
| Analytical Methods | p. 659 |
| Occurrence of NOC in Foods | p. 676 |
| Conclusions and Future Trends | p. 679 |
| Acknowledgements | p. 680 |
| References | p. 680 |
| Heterocyclic Amines | p. 685 |
| Introduction | p. 685 |
| Physical and Chemical Properties | p. 686 |
| Health Effects | p. 687 |
| Formation of Heterocyclic Amines | p. 688 |
| Food Sample Analysis | p. 689 |
| Occurrence in Food | p. 697 |
| Exposure Assessment | p. 700 |
| Regulations and Future Trends | p. 701 |
| Acknowledgements | p. 701 |
| References | p. 701 |
| Acrylamide, Chloropropanols and Chloropropanol Esters, Furan | p. 705 |
| Acrylamide | p. 705 |
| Chloropropanols and Chloroesters | p. 714 |
| Furan | p. 722 |
| Conclusion and Future Trends | p. 728 |
| References | p. 728 |
| Food Contact Materials | p. 733 |
| Introduction | p. 733 |
| Physical and Chemical Properties | p. 736 |
| Analytical Methods | p. 741 |
| Health Effects | p. 765 |
| Occurrence in Foods | p. 768 |
| Future Trends | p. 768 |
| References | p. 771 |
| Non-Target Multi-Component Analytical Surveillance of Food Contact Materials | p. 775 |
| Introduction | p. 776 |
| Legislation on Food Contact Materials | p. 776 |
| Non-Target Analysis | p. 778 |
| Examples of Non-Target Analysis from the Recent Literature | p. 782 |
| Safety Assessment of Migrants from FCM | p. 785 |
| Conclusions and Future Trends | p. 791 |
| References | p. 792 |
| List of Abbreviations | p. 795 |
| Subject Index | p. 807 |
| Table of Contents provided by Ingram. All Rights Reserved. |
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